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Thursday, December 19, 2013

#165 - Nova Analyzers from the Field – Episode 3

These pictures had us scratching our heads for a while. The analyzer installation is on a roof in South Africa at a plant that produces aluminum chlorohydrate. According to Wikipedia, aluminum chlorohydrate is used in deodorants and anti-perspirants and as a coagulant in water purification. This South African plant makes it in a reactor containing aluminum ingots, hot water, and aluminum chloride solution.



One by-product of the reaction is hydrogen and that is the gas they wanted to monitor on this site. Possibly because the concentration of H2 is an indicator of the pace of the reaction. High or low H2 content may trigger an adjustment in the addition rate of the aluminum chloride or the aluminum ingots.

The Nova analyzer is easy to identify. It’s the cabinet with the round port-hole, in the center of each picture. This is a Model 430N7MC Hydrogen analyzer with explosion-proof cabinet.

The other components attached to it were more difficult to identify. These were evidently the work of the original installer. From the site staff explanation, there is apparently a vortex-style cooler, a ‘silencer’, and a knock-out pot. We assume that the vortex cooler is intended to cool the gas and cause the moisture to condense and fall out in the knock-out pot. The ‘silencer’ is perhaps to regulate noise or velocity associated with the compressed air input (?). The intentions are good, but the implementation seemed questionable.

A vortex style cooler separates cold and hot fractions of air by spinning them very quickly. They require an input of compressed air in the side, and the hot and cold flows usually emerge from opposite ends of the tube. None of the components in the pictures seem to have that exact configuration. So we were uncertain about the correct operation of the installation.



We were also somewhat confused by the requirement for an explosion-proof analyzer. The components installed ahead of the analyzer do not seem to reflect this requirement.

Our concerns with the tubing layout and functionality of the parts were confirmed when it was revealed that the moisture system was not working properly and was allowing corrosion deposits to form in the system. The deposits were also apparently contributing to sporadic Low Flow alarms in the analyzer.

On the right side of the analyzer is a data collection cabinet or control device of some kind. The analyzer is equipped with a 4-20mA output corresponding to the range of gas analysis. This output is no doubt connected to the process control panel. Adjustments are automatically made in response to the hydrogen levels measured.

Last I heard, the plant was looking to resolve their installation problems and expand their chemical production capacity. It would make sense to tidy up the loose components and mount them on a common base plate with an upgraded tubing layout. Sourcing more reliable components may also be necessary.

Despite the questionable installation, we were glad to hear that the hydrogen analyzer was performing satisfactorily. If you have a requirement for H2 measurement in challenging applications, we can likely offer a solution for you too. Hydrogen page on Nova website.

Episode 1 - old portable flue gas with dual CO channel
Episode 2 - portable ppm H2 analyzer for university metallurgical lab


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Vortex tube graphic modified from:
http://en.wikipedia.org/wiki/Vortex_tube

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