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Showing posts with label gas analysis. Show all posts
Showing posts with label gas analysis. Show all posts

Wednesday, May 29, 2013

#124 - Particulate Removal from Sample Gases under Different Conditions

We have been using the heated filter concept for many years as an efficient way to extract a dusty gas sample and filter it prior to transportation to a gas analyzer. One of the reasons why we filter dusty applications at the extraction point is to avoid development of a dust / condensate slurry which would plug the sample tubing in and after the filter.

Our customers have had various combinations of conditions that have given rise to different configurations of heated filters as follows:
  1. The standard heated filter is attached to a flue gas duct using a mounting flange. This configuration is suitable for samples at basically atmospheric pressure. The installation must be in a non-hazardous area. The cabinet requires a supply of instrument air or nitrogen to allow a blowback of the filter and the probe. This pushes the accumulated dust back into the flue gas duct.
  2. The standard heated filter is also available in a hazardous area configuration. The heater is rated for hazardous areas and the electrical contacts are sealed in a small explosion-proof junction box.
  3. Some high pressure processes, such as Direct Reduction of Iron (DRI), also require dust removal before gas analysis. We can provide a high pressure configuration of the heated filter system. However, this system does not allow blowback because of the high pressure in the process.
  4. A version of the high pressure configuration is available that is suitable for hazardous areas.
  5. Some sample points on a DRI process are also quite hot. It may be necessary to cool the sample slightly before it enters the filter. We can provide water-cooled spool pieces that are mounted between the probe and the filter valve.
  6. We have also developed a vertical design which can be mounted on a duct or silo where the extraction probe is required to point downward into the gas atmosphere.



NOVA Heated filter system mounted vertically on a
process application at one of the US National Labs.
(Not our standard configuration, but worked
very well for this project.)

For information on these and other gas analyzer systems, give Mike or Dave at Nova a call, or send us an e-mail.
1-800-295-3771
sales at nova-gas dot com
websales at nova-gas dot com
http://www.nova-gas.com/

Thursday, February 7, 2013

#102 - Triple Point Analysis of Biogas at Palm Oil Facility

As Nova’s business has evolved over the years, we have noticed various trends with respect to customer requirements. One such trend is the gradual predominance of biogas inquires over landfill inquiries.

Anaerobic digester facility.

Excellent diagram of a full biogas system.

This is no doubt a reflection of the fact that new biogas projects are much more frequent than new landfill projects. Instead of paying to have their garbage hauled away to a landfill, many companies have preferred to invest in biogas systems that produce energy while reducing waste. Communities often push back on initiatives to start up large landfills in their regions, while they might be more favorable to biogas initiatives. Biogas projects are more tenable because they are smaller scale and do not consume large tracts of valuable land. By design, biogas digesters are covered and are therefore not as offensive to neighbors or attractive to vermin.


Land use of biogas vs. landfill


One such recent project involved one of our partners in Malaysia who is working with a customer to minimize waste effluent while recovering energy. The customer is in fact the largest palm oil producer in the world.*



The customer has an anaerobic digester and a gas scrubber. The requirement was to have analysis of methane (CH4) and hydrogen sulfide (H2S) at two points in the process – before and after the scrubber. The net result was that an analyzer system would be required to sample raw and cleaned biogas.

For this project, the customer also a requested a third sample point as follows:
1.     Raw biogas
2.     Scrubbed biogas
3.     Fresh air

The reason for points 1 & 2 is to determine the energy value of the produced gas, and to evaluate the efficacy of the scrubber. On these applications, there is often a stationary combustion engine of some kind which burns the produced methane. The engine will require input of at least a minimum methane content to function properly. Because methane is a strong greenhouse gas, it is often profitable for the stakeholders to know how much methane they are diverting from release into the atmosphere. Hydrogen sulfide is also a concern; if the H2S levels in the gas rise because of a scrubber failure, the engine will be damaged.

If a big heavy engine made out of hardened steel will be damaged by poorly cleaned gas, imagine what will happen to an analytical instrument that is continuously sampling the raw gas. To manage this reality, we have upgraded the valves, internal tubing, and other components in our biogas instruments to make them more durable.

This project required a 3-point sequencer and a gas analyzer. The sequencer automatically advances through the sample points in a cyclical pattern, spending a few minutes on each sample. The active sample is sent to the gas analyzer for analysis.

The third sample point mentioned above will be used by the customer to pump in clean air. The project stake-holders all agreed that this would be a good idea to increase sensor longevity. Even though H2S sensors are intended to be exposed to H2S, they will be consumed over time as their internal electrolyte is used up. This process will be accelerated if the sensor is exposed to high levels of H2S for long periods of time. To mitigate this process, we configured the sequencer to spend a few minutes sampling clean air after sampling the raw biogas. This will purge out the concentrated gas and ‘re-fresh’ the sensors.


The customer recently updated us with new information about the quality of their biogas. Apparently, it has a much higher moisture content than was originally expected. So they obtained a gas cooler which will be mounted ahead of the sequencer on the raw biogas stream. This will reduce the intensity of the gas that the sequencer will be exposed to during its operation.

We expect that we will continue to see an increase in biogas applications. We have also seen the same trend with syngas inquiries. The basic pattern of produced gas, gas cleaner, and combustion engine is frequently the same as with biogas.  (See this post.)

One additional point of analysis with both types of applications is at the exhaust of the combustion engine. Measuring the exhaust gases will help determine the operational health of the engine, and will determine the pollutant levels being emitted from the engine. Perhaps we can talk about this in a future post.

For information on gas analyzer systems, give Mike or Dave at Nova a call, or send us an e-mail.
1-800-295-3771
sales at nova-gas dot com
websales at nova-gas dot com


* Palm oil production is apparently an environmental issue because of its contribution to deforestation. See http://www.celsias.co.nz/article/true-costs-palm-oil-video/ and http://www.greenpeace.org/eastasia/campaigns/forests/work/palm-oil/

Deforestation resulting from development
of palm oil plantation.
Biogas system picture - http://www.unendlich-viel-energie.de/en/biomass/details/article/155/functioning-principles-of-a-biogas-system.html
Landfill site picture - http://www.co.stevens.wa.us/publicwrks/Landfill/landfill.htm
Biogas site picture - http://www.bbfm.de/1.html
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